Metrohm 833 IC Liquid Handling Unit - Handbuch (Seite 6)

Inhaltsverzeichnis
833 IC Liquid Handling Unit / Gebrauchsanweisung 8.833.1001
II
6.2 Anschluss an Modulares IC-System zur Kationenabtrennung ...............43
6.2.2 Einstellungen im IC Net.................................................................................... 47
6.3 Handhabung des Sample Preparation Moduls........................................49
7 IC Liquid Handling Dialysis Unit 833 ....................... 50
7.1 Ablaufschema für Dialyse .........................................................................51
7.2 Elektrischer Anschluss .............................................................................52
7.2.1 Dialyse ohne Suppression ............................................................................... 52
7.2.2 Dialyse mit Suppression .................................................................................. 53
7.3 Einstellungen in IC Net..............................................................................54
7.3.1 Dialyse ohne Suppression ............................................................................... 54
7.3.2 Dialyse mit Suppression .................................................................................. 55
7.4 Dialysezelle montieren ..............................................................................56
7.5 Kapillarverbindungen herstellen ..............................................................57
7.5.1 IC Separation Center 820 vorbereiten ............................................................. 57
7.5.2 Dialysezelle anschliessen ................................................................................ 58
7.6 Dialyse optimieren.....................................................................................63
7.6.1 Bestimmen der Spülzeit ................................................................................... 63
7.6.2 Bestimmen der Transferzeit ............................................................................. 63
7.6.3 Bestimmen der Dialysezeit............................................................................... 64
7.7 Vorgehen bei der Dialyse..........................................................................66
8 IC Liquid Handling Ultrafiltration Unit 833.............. 68
8.2 Ultrafiltrationszelle montieren...................................................................69
8.3 Filtrationszelle anschliessen ....................................................................70
8.4 Filtrieren .....................................................................................................74
8.4.1 Auswahl der möglichen Probenarten............................................................... 74
8.4.2 Filterstandzeiten ............................................................................................... 74
8.4.3 Auswahl der Filtrationsmembran ..................................................................... 75
9 Störungen - Wartung ................................................ 76
9.1 Störungen und deren Behebung ..............................................................76
9.2 Wartung und Unterhalt ..............................................................................79
9.2.1 Gerätepflege..................................................................................................... 79
9.2.2 Wartung durch Metrohm-Service..................................................................... 79
9.2.3 Stillegung.......................................................................................................... 79
9.2.4 Austausch der Pumpschläuche....................................................................... 80
9.2.5 Filter tauschen.................................................................................................. 81
9.2.6 Suppressor Modul / Sample Preparation Modul ............................................. 82
9.2.7 Dialysezelle....................................................................................................... 88
9.2.8 Ultrafiltrationszelle ............................................................................................ 90
10 Anhang ...................................................................... 91
10.1 Technische Daten......................................................................................91
10.1.1 Grundgerät 833 IC Liquid Handling Unit 1.833.0010 ...................................... 91
10.1.2 Dialysezelle 6.2729.100 ................................................................................... 94
10.1.3 Ultrafiltrationszelle 6.2729.110 ......................................................................... 94
10.2 Lieferumfang..............................................................................................95
10.2.1 IC Liquid Handling Pump Unit 833 .................................................................. 95
10.2.2 IC Liquid Handling Suppressor Unit 833 ......................................................... 96
10.2.3 IC Liquid Handling Sample Preparation Unit 833............................................ 97
10.2.4 IC Liquid Handling Dialysis Unit 833................................................................ 98
10.2.5 IC Liquid Handling Ultrafiltration Unit 833...................................................... 100